in neat (no solvent) Sn sulfide heating in 1,2-dibromoethane for 30 h at 140°C, solvent removing in vacuo; purified by sublimation in vacuo, identified by elem. anal.;
参考文献
Razuvaev, G.A.; Shcherbakov, V.I.; Grigor'Eva, I.K.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 245 - 252
triethylamine 1) 30 min, 115-120 deg C; 2) 2 h boiling in chlorobenzene; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Bondarenko, N. A.; Tsvetkov, E. N.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 7 p. 1533 - 1537,1361 - 1364