2-甲基-2,4-戊二醇合成路线 （共 135 条）
反应条件
T=200°C; Hydrogenation;
参考文献
Connor; Adkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 4680
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Schmerling; Friedman; Ipatieff
Journal of the American Chemical Society, 1940 , vol. 62, p. 2448
反应条件
in tetrahydrofuran T=14°C; Solvent;
参考文献
Tianjin Weijie Technology Co., Ltd.; SONG, Honghai; TANG, Long; CHEN, Wei; LI, Zheng; LI, Jinzhou; SUN, Zhicun; FENG, Jiajin
Patent: EP2662377 A1, 2013 ;
Location in patent: Paragraph 0031 ;
反应条件
cobalt(II) chloride in acetonitrile T=80°C; 5 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
CoCl2 in acetonitrile T=80°C; 3 h;
参考文献
Ahmad, Saeed; Iqbal, Javed
Journal of the Chemical Society, Chemical Communications, 1987 , # 2 p. 114 - 115
参考文献
Tryon
Journal of the American Chemical Society, 1947 , vol. 69, p. 972
反应条件
sodium methylate T=85°C; bei der Destillation;
参考文献
Standard Oil Devel.Co.
Patent: US2476053 , 1947 ;
反应条件
tetrakis(dimethylamino)diboron in toluene T=20 - 100°C; 1.25 h;
参考文献
BORON MOLECULAR PTY LTD
Patent: WO2004/76467 A1, 2004 ;
Location in patent: Page 15 ;
参考文献
The Commonwealth of Australia Commonwealth Scientific and Industrial Research Organization
Patent: US6346639 B1, 2002 ;
反应条件
potassium acetate in toluene T=80°C; 2 h;
参考文献
Bello, Charles S.; Schmidt-Leithoff, Joachim
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6230 - 6235,6
反应条件
1: 77 percent / p-TSA / benzene 2: 30 percent / aq. H2SO4 / hexane / 5 h / 20 °C View Scheme
参考文献
Kuznetsov; Brusilovskii, Yu E.
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 1 p. 138 - 139
