反应条件
water; acetic anhydride in tetrahydrofuran; toluene byproducts: tert-butanol, phenol; toluene soln. of peracetate, acetic anhydride, and Sb-compd. heating in evacuated tube (70°C, 35 h), liquid fraction condensing in cold trap, THF+H2O addn., liquid fraction condensing; solid residue extracting by hexane (removing SbPh3) and CHCl3 (product);elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 44, # 5 p. 937 - 940
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , # 5 p. 964 - 967