1: 1,1-bis(trifluoromethyl)-2-bromoethanol With n-butyllithium in diethyl ether; hexane
T=-78°C;
2: chloro-diphenylphosphine in diethyl ether; hexane
T=-78 - 20°C;
参考文献
Grushin, Vladimir V.; Marshall, William J.; Halliday, Gary A.; Davidson, Fredric; Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2002 , vol. 117, # 2 p. 121 - 129
1: n-butyllithium With methylenebis(diphenylphosphine oxide) in hexane
2: chloro-diphenylphosphine in hexane; benzene
10 h; Heating;
3: With dihydrogen peroxide in diethyl ether; acetone
参考文献
Pisareva; Petrovskii; Lyssenko; Antipin; Nifant'ev
Russian Chemical Bulletin, 2004 , vol. 53, # 9 p. 2008 - 2012