triisopropylstibane in neat (no solvent)
(N2); std. Schlenk technique; according to Bulten E. J., et al., J. Organomet. Chem., 1976, 117, 329; suspn. of SnBr2, dibromopropane and Et3Sb was slowly warmed to 155°C within 45 min and stirred for 5 h; dibromopropane removed (vac.); distd.; elem. anal.;
参考文献
Schumann, Herbert; Aksu, Yilmaz; Wassermann, Birgit C.
Organometallics, 2006 , vol. 25, # 14 p. 3428 - 3434
Yanagawa, Makato; Moriya, Osamu; Watanabe, Yoshihiko; Ueno, Yoshio; Endo, Takeshi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 2203 - 2204
