Ehn, Marcel; Vassilev, Nikolay Georgiev; Kasak, Peter; Horvath, Branislav; Filo, Juraj; Mereiter, Kurt; Rakovsky, Erik; Putala, Martin
Tetrahedron Asymmetry, 2013 , vol. 24, # 20 p. 1303 - 1311
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反应条件
1: 2',2'-dibromocycloprop-1'-yloxirane; n-butyllithium in diethyl ether; hexane T=-75 - 20°C; 2.5 h; 2: methanesulfonyl chloride With triethylamine in dichloromethane T=-35 - -30°C; 1.5 h; Title compound not separated from byproducts;
参考文献
Bentley, T. William; Engels, Bernd; Hupp, Thomas; Bogdan, Elena; Christl, Manfred
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1018 - 1026
1: 2',2'-dibromocycloprop-1'-yloxirane; n-butyllithium in diethyl ether; hexane T=-75 - 20°C; 2.5 h; 2: methanesulfonyl chloride With triethylamine in dichloromethane T=-35 - -30°C; 1.5 h; 3: With water; triethylamine in acetone T=22°C; 18 h; Title compound not separated from byproducts;
参考文献
Bentley, T. William; Engels, Bernd; Hupp, Thomas; Bogdan, Elena; Christl, Manfred
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1018 - 1026
