反应条件
in benzene
Schlenk techniques; V compd. (1.1 mmol) in benzene mixed with iodide (4.54 mmol), stirred at 80°C for 10 h; filtered, solvent evapd., extd. (hexane), evapd., sublimed (100-110°C, 0.1 Torr); residue after extn. recrystd. (THF);
参考文献
Burin, Mikhail E.; Smirnova, Marina V.; Fukin, Georgy K.; Baranov, Eugeny V.; Bochkarev, Mikhail N.
European Journal of Inorganic Chemistry, 2006 , # 2 p. 351 - 356
