乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
sodium acetate in chloroform
4 h; Reflux;
参考文献
Harris, Geraint H.; Graham, Andrew E.
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6890 - 6892
参考文献
Mawaziny, Sheila; Makky, Sadiah
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 167, p. 61 - 69
反应条件
1: α,α'-dihydroxy-p-xylene With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene in dichloromethane
T=20°C; 7 h;
2: ethyl (triphenylphosphoranylidene)acetate in dichloromethane
T=20°C; Wittig reaction; 1 h;
参考文献
Vatele, Jean-Michel
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 715 - 718
反应条件
manganese(IV) oxide in chloroform
Oxidation; Wittig reaction; 20 h; Heating;
参考文献
Blackburn, Leonie; Wei, Xudong; Taylor, Richard J. K.
Chemical Communications, 1999 , # 14 p. 1337 - 1338
反应条件
in dichloromethane
T=20°C;
参考文献
Yang; Jiao; Yip; Lai; Wong
Journal of Organic Chemistry, 2001 , vol. 66, # 13 p. 4619 - 4624
反应条件
1: in toluene
T=20°C; 0.25 h;
2: With sodium methylate in methanol
T=20°C; 20 h; Reflux;
3: With hydrogenchloride in ethanol; water
参考文献
Chen, Yuan-Siao; Yu, Hui-Ming; Shie, Jiun-Jie; Cheng, Ting-Jen Rachel; Wu, Chung-Yi; Fang, Jim-Min; Wong, Chi-Huey
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 5 p. 1766 - 1772
反应条件
T=50°C; P=6750540 Torr; 35 h;
参考文献
Isaacs, Neil S.; El-Din, Ghazi Najim
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2191 - 2192
反应条件
in N,N-dimethyl-formamide
0.5 h; Ambient temperature;
参考文献
Rauter, Amelia P.; Figueiredo, Jose A.; Ismael, Isabel M.
Carbohydrate Research, 1989 , vol. 188, p. 19 - 24
反应条件
in chloroform
6 h; Heating;
参考文献
Chordia, Mahendra D.; Narasimhan, Nurani S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 371 - 376
反应条件
1: 94 percent / CHCl3 / 8 h / Heating
2: 78 percent / 2N NaOH / H2O; benzene / 25 °C
View Scheme
参考文献
Mali, Raghao S.; Tilve, Santosh G.; Yeola, Suresh N.; Manekar, Anita R.
Heterocycles, 1987 , vol. 26, # 1 p. 121 - 127
