sodium hydroxide in water
diol-to-B-compd. ratio 1.29, 1.58, or 2.00; products not isolated, reaction monitoring by NMR;
参考文献
Shvarts, E. M.; Kamars, A. E.
Russian Journal of General Chemistry, 1997 , vol. 67, # 5 p. 687 - 689
Zhurnal Obshchei Khimii, 1997 , vol. 67, # 5 p. 735 - 737
in neat (no solvent)
H3BO3:melamine were mixed in 2:1 ratio, heating at 200 and 300 °Cfor 1 and 2 h, resp., cooling, pulverizing, powder was put into a furna ce heated up to 1600 °C for 15 min; detn. by XPS;
in water
Kinetics; Electrochem. Process; CuSO4 soln. added to H3BO3 and citric acid soln., pH regulated by addition KOH or H2SO4, at room temp.; detd. by HRSEM and XRD;
参考文献
Cohen-Hyams; Kaplan; Aurbach; Cohen; Yahalom
Journal of the Electrochemical Society, 2003 , vol. 150, # 1 p. C28-C35
Paushkin, Ya. M.; Panidi, I. S.
Tr. Mosk. Inst. Neftekhim. i Gaz. Prom., 1963 , # 44 p. 33 - 38
C.A., 1964 , vol. 60, p. 10189
Full Text Show Details
Gmelin Handbook: B: B-Verb.4, 4.5.3.1, page 138 - 138
