in tetrahydrofuran addn. of CH2Cl2 to soln. of B-methoxyborecane in THF, cooling to -78°C, slow addn. of sec-BuLi over period of 0.5 h, stirred at -78°C for 0.25 h, addn. of KIPBH, warmed to room temp, stirred for 14 h;; GLC, amt. of cyclodecanol formed depends upon temp. during the addn. of KIPBH;;
参考文献
Journal of the American Chemical Society, , vol. 110, # 18 p. 6263 - 6264
