N,N-二甲基-2-苯乙胺合成路线 (共 89 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 10 h; Heating; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 45, # 4 p. 613 - 617
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 10 h; Heating; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 45, # 4 p. 613 - 617
反应条件
lithium aluminium tetrahydride in diethyl ether 3 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 3 p. 616 - 622
反应条件
1: dimethyl amine With n-butyllithium in tetrahydrofuran; hexane T=-50 - -12°C; 2 h; 2: 1-(1-phenylvinyl)-1-silacyclohexane in tetrahydrofuran; hexane T=-30 - 4°C; 19 h;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 17 p. 3589 - 3595
反应条件
sulfuric acid; As2O3 T=40°C; Electrolysis.an Bleikathoden;
参考文献
Chemische Berichte, , vol. 56, p. 2063
Chemische Berichte, , vol. 57, p. 774
Archiv der Pharmazie (Weinheim, Germany), , p. 390,400
Chem. Zentralbl., , vol. 95, # II p. 1404
反应条件
2: 99 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 44 p. 5367 - 5370
反应条件
ammonia; sodium in tetrahydrofuran T=-78°C; 0.0833333 h; regioselective reaction;
参考文献
Tetrahedron, , vol. 65, # 16 p. 3232 - 3238
反应条件
1: phenethylamine 2: methyl iodide in dichloromethane 3: With sodium acetate; acetic acid T=100°C;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 1 p. 5 - 8
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Synthetic Communications, , vol. 3, p. 325 - 332
反应条件
1: carbon dioxide; phenethylamine With caesium carbonate in N,N-dimethyl-formamide T=23°C; 0.75 h; 2: methyl iodide in N,N-dimethyl-formamide T=23°C; 8 h;
参考文献
Tetrahedron, , vol. 58, # 17 p. 3329 - 3347