119072-55-8合成路线 （共 225 条）
反应条件
cesium fluoride in acetonitrile
T=30°C; 24 h; Inert atmosphere;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
in dichloromethane
T=20°C; 24 h;
参考文献
Yavari, Issa; Djahaniani, Hoorieh; Nasiri, Farough
Synthesis, 2004 , # 5 p. 679 - 682
反应条件
water in dichloromethane
T=20°C; 0.333333 h;
参考文献
Shaabani, Ahmad; Soleimani, Ebrahim; Hossein Rezayan, Ali
Tetrahedron Letters, 2007 , vol. 48, # 12 p. 2185 - 2188
反应条件
hydrogenchloride in acetonitrile
4 h; Heating;
参考文献
Charrier, Josiane; Foucaud, Andre'; Person, Herve'; Loukakou, Emile
Journal of Organic Chemistry, 1983 , vol. 48, # 4 p. 481 - 486
反应条件
1: tert-butylisonitrile; phenylacetylene With Ti(NMe2)2(dpma); cyclohexylamine in toluene
T=100°C; 24 h; Inert atmosphere;
2: benzenecarboximidamide hydrochloride in 1,1-dimethylpropan-1-ol
T=145 - 150°C; 24 h; Inert atmosphere;
参考文献
Majumder, Supriyo; Odom, Aaron L.
Tetrahedron, 2010 , vol. 66, # 17 p. 3152 - 3158
反应条件
titanium tetrachloride in dichloromethane
T=0°C;
参考文献
Ito, Yoshihiko; Kato, Hidehito; Imai, Hiroshi; Saegusa, Takeo
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6449 - 6450
反应条件
2,4-di-Nitrobenzene in benzene
T=20°C; Addition; 24 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
in tetrahydrofuran
addn. of t-butylisocyanide to a suspn. of bis(O,O-2,5 -diphenyl-1,3,2,5-dioxaboraphosphorinane) copper(I) iodide, standing for 6 h; filtn., evapn. of the filtrate, recrystn. from ethyl ether;
参考文献
Arbuzov, B. A.; Nikonov, G. N.; Karasik, A. A.; Enikeev, K. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 4.2 p. 804 - 809
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 4 p. 906 - 912
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene
2 h; RefluxInert atmosphere;
参考文献
Boissarie, Patrick J.; Hamilton, Zoe E.; Lang, Stuart; Murphy, John A.; Suckling, Colin J.
Organic Letters, 2011 , vol. 13, # 23 p. 6256 - 6259
反应条件
1: With Ti(N(CH3)2)2(CH2(C4H3N)2); (3,5-dichlorophenyl)-(7-methoxymethyl-[1,4]-dioxano[2,3-g]quinazolin-4-yl)-amine in toluene
T=100°C; 48 h; Inert atmosphere;
2: With hydroxylamine hydrochloride in tetrahydrofuran; toluene
T=45°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Dissanayake, Amila A.; Odom, Aaron L.
Tetrahedron, 2012 , vol. 68, # 3 p. 807 - 812
