反应条件
1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 5 h / 0 - 20 °C / |Inert atmosphere 1.2: 16 h / 60 °C 2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 22 h / 40 °C / |Inert atmosphere 2.2: |Acidic conditions; |Inert atmosphere 3.1: oxygen / N,N-dimethyl-formamide / 16 h / 60 °C 3.2: |Acidic conditions View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 20 p. 10405 - 10413