in hexane Irradiation (UV/VIS); photochemical react. of Co2(CO)8 with cyclopentadiene in hexane at room temp. according to King, R. B. (1965). Organometallic Synthesis. Vol. 1, pp. 118-119. New York: Academic Press.;
in toluene soln. of Co complex in toluene was added with stirring to suspn. of Zr complex and oxirane in toluene at 20°C under Ar; stirred; IR monitoring; not isolated;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 9 p. 1817 - 1824
in toluene Schlenk technique; suspn. of Ti complex and Co complex in toluene was stirred at -40°C for 10 min under CO; oxirane was added; mixt. was stirred at -40°C for 30 min; slowly warmed to 20°C; stirred for 3 h; IR monitoring; not isolated;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 9 p. 1817 - 1824
Kinetics; Flowing afterglow app., He buffer gas (0.5 Torr), 298 K, radical anion generated by electron impact on corresponding neutral complex, neutral ligand substrate was added to the helium flow.; Ion compn. of the flow monitored with quadrupole mass filter and electron multiplier.;
Kinetics; Flowing afterglow app., He buffer gas (0.5 Torr), 298 K, radical anion generated by electron impact on corresponding neutral complex, neutral ligand substrate was added to the helium flow.; Ion compn. of the flow monitored with quadrupole mass filter and electron multiplier.;
Kinetics; Flowing afterglow app., He buffer gas (0.5 Torr), 298 K, radical anion generated by electron impact on corresponding neutral complex, neutral ligand substrate was added to the helium flow.; Ion compn. of the flow monitored with quadrupole mass filter and electron multiplier.;