反应条件
in benzene dropwise addn. of phosphine to Rh-compound in benzene (N2, Schlenk tube technique), stirring for 1h at room temp., filtn., washing with ether, drying in vac., dissolving in methanol, addn. of NH4PF6, stirring for 10 min; addn. of ether, filtn., washing with ether, recrystn. (acetone/ether);
参考文献
Werner, Helmut; Hofmann, Lothar; Paul, Wilfried; Schubert, Ulrich
Organometallics, 1988 , vol. 7, p. 1106 - 1111
