in dichloromethane CH2Cl2 soln. (CpCo(dpae)I)I reacted with P(OCH3)3 with stirring for 1 h; solvent removed, solid chromed. on silica with CH2Cl2 and acetone;
参考文献
Landon, Shayne J.; Brill, Thomas B.
Inorganic Chemistry, 1984 , vol. 23, p. 1266 - 1271
→
反应条件
T=23 - 25°C; 2 h;
参考文献
Russian Journal of General Chemistry, , vol. 73, # 11 p. 1738 - 1741