1227476-15-4合成路线 (共 213 条)
反应条件
in toluene Ti-complex was suspended in toluene, treated with ligand, stirred for 24 h under N2; mixt. was concd., heptane was added, solid filtered off, obtained TiCl2(cp)2, cooled soln. to -78°C obtained Ti(cp)2(PhNNPh);
参考文献
Fochi, Giovanni; Floriani, Carlo; Bart, Jan C. J.; Giunchi, Giovanni
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1515 - 1522
反应条件
sulfuric acid; orthoarsenic acid; glycerol
参考文献
Matsumura
Journal of the American Chemical Society, 1930 , vol. 52, p. 3974,3976
反应条件
T=100°C; im geschloseenen Rohr;
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 35, p. 667
Chem. Zentralbl., , vol. 74, # II p. 1270
反应条件
T=368.9 - 437.4°C; 0.5 h; var. system, initial conc., temp., time, surface-to-volume ratio, additives; Kinetics;
参考文献
Barton, Donald; Hodgett, Michael; Skirving, Paul; Whelton, Michael; Winter, Keith; Vardy, Cathy
Canadian Journal of Chemistry, 1983 , vol. 61, p. 1712 - 1718
反应条件
pyridine; iron tribromide; Rhodium trichloride; 1,2-dichloro-4-nitrobenzene; p-methylnitrobenzene; vanadium pentoxide in chlorobenzene T=175°C; P=60004.8 Torr; 1 h; other reagents; Product distribution;
参考文献
Manov-Yuvenskii, V. I.; Petrovskii, K. B.; Lapidus, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2486 - 2489
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2717 - 2721
参考文献
Wislicenus; Eichert; Marquardt
Justus Liebigs Annalen der Chemie, 1924 , vol. 436, p. 93
参考文献
Organometallics, , vol. 25, # 13 p. 3111 - 3113
反应条件
sodium perborate in acetic acid T=50 - 60°C; 2 h;
参考文献
McKillop, Alexander; Tarbin, Jonathan A.
Tetrahedron, 1987 , vol. 43, # 8 p. 1753 - 1758
反应条件
(C3F7CO2)2 in dichloromethane; 1,2,2-trifluoro-trichloroethane T=0°C; 8 h;
参考文献
Matsui, Masaki; Kawamura, Shigeo; Shibata, Katusoyoshi; Muramatsu, Hiroshige; Mitani, Motohiro; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 209 - 217
反应条件
in dichloromethane; 1,2,2-trifluoro-trichloroethane T=0°C; 8 h;
参考文献
Matsui, Masaki; Kawamura, Shigeo; Shibata, Katusoyoshi; Muramatsu, Hiroshige; Mitani, Motohiro; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 209 - 217