1227476-15-4合成路线 （共 213 条）
反应条件
samarium diiodide in tetrahydrofuran T=65°C; 0.2 h;
参考文献
Li, Xue; Zhang, Yongmin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 6 p. 1576 - 1578
参考文献
Tichwinski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1903 , vol. 35, p. 667
Chem. Zentralbl., 1903 , vol. 74, # II p. 1270
反应条件
carbon monoxide; anhydrous lithium acetate; triphenylphosphine; ruthenium trichloride in various solvent(s) T=180°C; 8 h; amount of base and alcohol; substituents at 4,4' positions of azobenzene; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 295, p. 91 - 98
参考文献
Siebert,W.; Ospici,A.
Chemische Berichte, 1972 , vol. 105, p. 454 - 463
反应条件
1.1: hydrazine hydrate / ethanol / 0.5 h / 60 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 - -60 °C / Inert atmosphere 2.2: 1 h / -60 - 20 °C / Inert atmosphere 3.1: titanium(III) chloride; water / tetrahydrofuran / pH 10 / Reflux; Alkaline aq. solution; Inert atmosphere View Scheme
参考文献
Zhang, Yan; Tang, Qiang; Luo, Meiming
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 13 p. 4977 - 4982
反应条件
T=100°C; im geschloseenen Rohr;
参考文献
Tichwinski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1903 , vol. 35, p. 667
Chem. Zentralbl., 1903 , vol. 74, # II p. 1270
参考文献
Gilman; Pickens
Journal of the American Chemical Society, 1925 , vol. 47, p. 2408
参考文献
Werigo
Justus Liebigs Annalen der Chemie, 1865 , vol. 135, p. 178
Justus Liebigs Annalen der Chemie, 1873 , vol. 165, p. 199
参考文献
Werigo
Justus Liebigs Annalen der Chemie, 1865 , vol. 135, p. 178
Justus Liebigs Annalen der Chemie, 1873 , vol. 165, p. 199
参考文献
Merck and Co. Inc.
Patent: US2489927 , 1946 ;
