反应条件
in hexane addn. of C3O2 to AlMe3 (1:2, hexane) under stirring at -78°C, warming to room temp., standing for 10 h; cooling to -30°C and hydrolysing with NH4Cl-NH3-buffer (pH 8), sepn. of the organic layer, evapn. (vac.) and distn.;
参考文献
Gazzetta Chimica Italiana, , vol. 119, # 1 p. 59 - 62
