1: 3-bromo-1-(trimethylsilyl)-1-propyne With manganese; bis(8-quinolinolato) chromium chloride in tetrahydrofuran T=20°C; 0.5 h; 2: Caprylic Aldehyde With triethylsilyl chloride in tetrahydrofuran T=20°C; 60 h; 3: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; Title compound not separated from byproducts;
参考文献
Xia, Guoyao; Yamamoto, Hisashi
Journal of the American Chemical Society, 2007 , vol. 129, # 3 p. 496 - 497