carbon monoxide; nitrogen; magnesium in tetrahydrofuran byproducts: MgCl2; further reagents; an excess of Mg turnings was added with stirring to aTHF soln. of Cp2TiCl2 under N2, after 24 h the mixt. was left under CO for 5 h with stirring, evapd. in vacuo, residue was treated with MeI in a sealed ampoule for 24 h at 373 K; GLC and IR spectral data;
参考文献
Sobota, Piotr; Janas, Zofia
Journal of Organometallic Chemistry, 1983 , vol. 243, # 1 p. 35 - 44
Markovskii, L. N.; Tovstenko, V. I.; Martynyuk, E. G.; Pashinnik, V. E.; Shermolovich, Yu. G.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 3.1 p. 516 - 520,422 - 425
Foss, V. L.; Semenenko, N. M.; Sorokin, N. M.; Lutsenko, I. F.
Journal of Organometallic Chemistry, 1974 , vol. 78, p. 107 - 113
Full Text View citing articles Show Details
Gmelin Handbook: Sb: Org.Comp.2, 1.2.1.1.11.1, page 40 - 44
