反应条件
in thionyl chloride under Ar, 3 h, 90°C, stirring, addn. of further SO2Cl2, reflux for further 3 h; partial evapn., several d at -25°C, decantation, washing (pentane, ether), pulverizing, heating several h (vac., 50 °C); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 421, # 2-3 p. 215 - 231
