N,N-二甲基二茂铁甲胺合成路线 （共 30 条）
反应条件
ammonium chloride; mercury dichloride in water room temp.;
参考文献
Ratajczak, A.; Czech, B.; Misterkiewicz, B.
Bull. Acad. Polon. Sci. Ser. Sci. Chim., 1977 , vol. 25, p. 541 - 544
C.A., 1978 , vol. 88, p. 37943
Full Text Show Details
Gmelin Handbook: Fe: Org.Verb.A4, 5.1.4.1.3.2.1, page 42 - 44
反应条件
B(C2H5)3 in benzene-d6 Ar; Et3b added with stirring to a soln. of Pb comp. at room temp.; detected by NMR;
参考文献
Organometallics, , vol. 19, # 7 p. 1438 - 1441
反应条件
in acetic acid in boiling glacial acetic acid;;
参考文献
Fe: Org.Verb.A1, 2.5.7.10, page 166 - 167
Journal of Organic Chemistry, , vol. 21, p. 382 - 383
Journal of Organic Chemistry, , vol. 22, p. 355 - 358
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1631 - 1635
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1776 - 1782
反应条件
acetic acid 5 h; Reflux;
参考文献
Tarasova, Ol'Ga A.; Tatarinova, Inna V.; Vakul'Skaya, Tamara I.; Khutsishvili, Spartak S.; Smirnov, Vladimir I.; Klyba, Lyudmila V.; Prozorova, Galina F.; Mikhaleva, Al'Bina I.; Trofimov, Boris A.
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 1 - 7
反应条件
n-butyllithium in tetrahydrofuran; diethyl ether a mixt. of monodeuteroamines was reacted with an ethereal soln. of n-BuLi in ether-THF at 24°C, treated with D2O;
参考文献
Journal of Organometallic Chemistry, , vol. 202, # 2 p. 201 - 210
反应条件
sodium tetrahydroborate in diethyl ether; ethanol soln. of Fe complex in Et2O added to suspn. of NaBH4 in EtOH, mixture stirred for 0.5 h, poured into H2O; extn. (Et2O), washing with H2O, drying over MgSO4, evapn.;
参考文献
Cully, Norman; Watts, William E.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1981 , vol. 11, p. 695 - 705
反应条件
in tetrahydrofuran 12 equiv of borane, THF, reflux, 1 h or 18 h;
参考文献
Journal of Organometallic Chemistry, , vol. 637-639, p. 364 - 371
反应条件
in diethyl ether addn. of HgCl2 in portions to ferrocenyl Li complex suspn. with stirring, room temp., 40 h; addn. of water; stirring, 3h; separation of ether layer; extraction of aq. phase (three times with diethylether); washing of ether phases with water; drying; distn. off ether; heating in vac. (2 Torr); subl. of Hg cpd.; all operations under argon;
参考文献
Krueger, Christian; Thiele, Karl-Heinz; Dargatz, Manfred; Bartik, Tamas
Journal of Organometallic Chemistry, 1989 , vol. 362, p. 147 - 154
参考文献
Bulletin de la Societe Chimique de France, , p. 2656 - 2665
Fe: Org.Verb.A4, 5.1.4.1.3.2.1, page 42 - 44
Proc. 4th Intern. Conf. Organometal. Chem., Bristol 1969, G3
