2,6-二叔丁基-4-甲基苯酚合成路线 (共 290 条)
反应条件
1-butyl-3-methylimidazolium heptachlorodiindate (III) T=100°C; 1.5 h; In ionic liquid; Product distribution / selectivity;
参考文献
WO2006/74401 A1, ;
Page/Page column 25 ;
反应条件
methanol; trifluoroacetic acid T=30°C; 1.85 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 3 p. 858 - 867
反应条件
methanol; sodium hydroxide; formaldehyd T=225°C;
参考文献
US2841623 , ;
US2841624 , ;
反应条件
(3,5-di-tert-butyl-4-oxo-2,5-cyclohexadien-1-ylidene)-(3,5-di-tert-butyl-4-hydroxyphenyl)methane in benzene T=24.9°C; Equilibrium constant;
参考文献
Journal of Organic Chemistry, , vol. 59, # 17 p. 5063 - 5070
反应条件
methanol; trifluorormethanesulfonic acid T=30°C; 0.35 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 3 p. 858 - 867
反应条件
methanol T=30°C; 2.08333 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 3 p. 858 - 867
反应条件
sodium methylate T=200°C;
反应条件
in hexane T=30°C; 1 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 3 p. 921 - 927
反应条件
tetrapolyphosphoric acid T=40°C;
反应条件
LDP in diethyl ether 24 h; Ambient temperatureother conditions; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 36, # 88 p. 2137 - 2140