3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1: 68 percent / Li2CuCl4 / tetrahydrofuran / 0 - 20 °C 2: 60 percent / Mn; 2,4,6-collidine; Me3SiCl / Cp2TiCl2 / tetrahydrofuran / 20 °C 3: 76 percent / DMAP / CH2Cl2 / 2 h / 20 °C 4: 77 percent / AIBN; HSnBu3 / benzene / 1 h / Heating View Scheme
参考文献
Gansaeuer, Andreas; Justicia, Jose; Rosales, Antonio; Worgull, Dennis; Rinker, Bjoern; Cuerva, Juan Manuel; Oltra, Juan Enrique
European Journal of Organic Chemistry, 2006 , # 18 p. 4115 - 4127
反应条件
2: tin; aq.-ethanolic HCl; CuSO4 View Scheme
参考文献
Jenkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 1155,1161
参考文献
Baciocchi, Enrico; Bietti, Massimo; Putignani, Lorenza; Steenken, Steen
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5952 - 5960
反应条件
1: cadmium chloride; diethyl ether; benzene / Erwaermen der vom Aether befreiten Reaktionsloesung mit Bernsteinsaeure-methylester-chlorid 2: ethanolic KOH-solution View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2877
反应条件
diethyl ether; benzene Erwaermen des nach der Hydrolyse erhaltenen Reaktionsproduks mit Aethanol;
参考文献
Journal of the Chemical Society, , p. 431
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=0°C;
参考文献
Duplais, Christophe; Bures, Filip; Sapountzis, Ioannis; Korn, Tobias J.; Cahiez, Gerard; Knochel, Paul
Angewandte Chemie - International Edition, 2004 , vol. 43, # 22 p. 2968 - 2970
反应条件
1: 19 percent / potassium 12-tungstocobalt(III)ate; sodium tartrate buffer / H2O / 48 h / pH 4.0 View Scheme
参考文献
Bietti, Massimo; Lanzalunga, Osvaldo
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2632 - 2638
反应条件
iron(III) chloride amine-bis(phenolate) complex in diethyl ether; dichloromethane 0.5 h;
参考文献
Chemical Communications, , # 1 p. 94 - 96
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; diethyl ether T=20°C; 2 h; oth. Pd catalyst; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 7 p. 1222 - 1231
Zhurnal Organicheskoi Khimii, , vol. 23, # 7 p. 1354 - 1364
反应条件
C68H72Cl2N6NiP2 in tetrahydrofuran T=50°C; 12 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2011 , vol. 17, # 18 p. 4972 - 4975
