反应条件
in acetonitrile
byproducts: HCl, SiF4; gently refluxing KHF2 suspension; addn. of SO2Cl2 soln. with stirring during 1h; refluxing, 1h; condensing into trap at liq. nitrogen temp.; distn., -100°C; distn., -50°C; separation of SO2ClF; addn. of HI to distillate; passing through KMnO4 soln.; drying over P2O5; storage in a glass globe; elem. anal.;
参考文献
Padma, D. K.; Bhat, V. Subrahmanya; Murthy, A. R. Vasudeva
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1981 , vol. 20, p. 777 - 779
