2,2-二溴-1-苯乙酮合成路线 (共 82 条)
反应条件
1: With potassium phosphate; sodium iodide in sulfolane T=20 - 35°C; Inert atmosphere; 2: With tert.-butylhydroperoxide in sulfolane; decane T=30 - 35°C; Inert atmosphere;
参考文献
Synlett, , vol. 23, # 7 p. 1013 - 1020
反应条件
carbon tetrabromide; water; oxygen 10 h; Irradiation;
参考文献
Synlett, , vol. 24, # 5 art. no. ST-2013-U0018-L, p. 607 - 610
参考文献
Kroehnke
Chemische Berichte, 1933 , vol. 66, p. 1386,1391
Chemische Berichte, 1950 , vol. 83, p. 50,56
参考文献
Engler; Hassenkamp
Chemische Berichte, 1885 , vol. 18, p. 2241
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Pinner; Franz
Chemische Berichte, 1905 , vol. 38, p. 1533
反应条件
potassium hydroxide racemic mandelic acid;
参考文献
Engler; Woehrle
Chemische Berichte, 1887 , vol. 20, p. 2202
参考文献
Aston et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1413,1414
反应条件
tert.-butyl lithium; lithium hexamethyldisilazane Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kowalski, Conrad J.; Fields, Kevin W.
Journal of the American Chemical Society, 1982 , vol. 104, # 1 p. 321 - 323
反应条件
mercury dichloride; zinc in diethyl ether; ethyl acetate T=55 - 60°C; 0.5 h;
参考文献
Shchepin, V. V.; Gladkova, G. E.; Russkikh, N. Yu.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 6.1 p. 902 - 907
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 6 p. 1156 - 1162
参考文献
Aston et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1413,1414
参考文献
Madelung; Oberwegner
Justus Liebigs Annalen der Chemie, 1931 , vol. 490, p. 201,210, 225
Justus Liebigs Annalen der Chemie, 1936 , vol. 526, p. 195,230