136918-14-4合成路线 （共 708 条）
反应条件
T=100°C; bei mehrstuendigem Erhitzen;
参考文献
Chemische Berichte, , vol. 31, p. 3234
参考文献
Justus Liebigs Annalen der Chemie, , vol. 510, p. 62,69
反应条件
tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 116, # 1 p. 1 - 5
反应条件
1: 63 percent / PPh3, diethyl azodicarboxylate / tetrahydrofuran / 1.) -10 deg C, 3 h, 2.) 22 deg C, 15 h 2: 99 percent / trifluoroacetic acid / methanol / 1.) 22 deg C, 24 h, 2.) reflux, 3 h 3: 70 percent / lead tetraacetate / benzene / 0.5 h / 22 °C 4: 67 percent / Jones' reagent / acetone / 0 °C View Scheme
参考文献
Mulzer, Johann; Angermann, Alfred; Schubert, Boris; Seilz, Carsten
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5294 - 5299
参考文献
Mesropyan; Ambartsumyan; Avetisyan; Galstyan
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 6 p. 650 - 653
反应条件
[Ru4H6(p-cumene)4]Cl2; hydrogen in water T=90°C; P=45003.6 Torr; 24 h;
参考文献
Aoun, Rimane; Renaud, Jean-Luc; Dixneuf, Pierre H.; Bruneau, Christian
Angewandte Chemie - International Edition, 2005 , vol. 44, # 13 p. 2021 - 2023
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; hydrogen in water T=50°C; P=45003.6 Torr; 23 h;
参考文献
Aoun, Rimane; Renaud, Jean-Luc; Dixneuf, Pierre H.; Bruneau, Christian
Angewandte Chemie - International Edition, 2005 , vol. 44, # 13 p. 2021 - 2023
参考文献
Aventis Pharma Deutschland GmbH
Patent: US2004/6119 A1, 2004 ;
Location in patent: Page/Page column 22 ;
US 20040006119 A1
参考文献
Anselmi, Cecilia; Catelani, Giorgio; Monti, Luigi
Gazzetta Chimica Italiana, 1984 , vol. 114, # 5/6 p. 205 - 210
反应条件
potassium carbonate in N,N-dimethyl-formamide 12 h; Heating;
参考文献
Feller, Dennis R.; Miller, Duane D.
Patent: US2004/19079 A1, 2004 ;
Location in patent: Page/Page column 27 ;
US 20040019079 A1
