136918-14-4合成路线 (共 708 条)
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
反应条件
hydrazine hydrate; triphenylphosphine in tetrahydrofuran; methanol; water; acetic acid
参考文献
KNOLL Aktiengesellschaft
Patent: US5780642 A1, 1998 ;
反应条件
1: methanol With iodobenzene; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid T=0°C; 0.166667 h; Inert atmosphere; 2: phthalimide With potassium carbonate T=0 - 20°C; Hofmann-type rearrangement; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Organic Letters, , vol. 14, # 3 p. 946 - 949
反应条件
potassium carbonate in methanol; N-methyl phthalimide
参考文献
Enichem S.p.A.
Patent: US5780645 A1, 1998 ;
反应条件
hexaammonium heptamolybdate tetrahydrate T=120°C; 0.166667 h; Microwave irradiation;
参考文献
Seyyedhamzeh, Mozhdeh; Ganji, Nasim; Shaabani, Ahmad
Journal of Porphyrins and Phthalocyanines, 2012 , vol. 16, # 10 p. 1110 - 1113
反应条件
iron sulphate heptahydrate; ammonium molibdate; urea 0.05 h; HeatingMicrowave irradiation;
参考文献
Kumar, Vishal; Sharma, Upendra; Verma, Praveen K.; Kumar, Neeraj; Singh, Bikram
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 870 - 878
反应条件
in water T=100°C; 4 h;
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
in 1,1,2,2-tetrachloroethylene T=110°C; 8 h;
参考文献
Quan, Zheng-Jun; Ren, Rong-Guo; Jia, Xiao-Dong; Da, Yu-Xia; Zhang, Zhang; Wang, Xi-Cun
Tetrahedron, 2011 , vol. 67, # 13 p. 2462 - 2467
反应条件
sodium methylate 1.) electrolysis, current density 0.05 A/cm2, 2 h, 2.) electrolysis, current density 0.02 A/cm2, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Orzeszko, Andrzej; Maurin, Jan K.; Niedzwiecka-Kornas, Anna; Kazimierczuk, Zygmunt
Tetrahedron, 1998 , vol. 54, # 26 p. 7517 - 7524
参考文献
Sachs
Chemische Berichte, 1898 , vol. 31, p. 3234
Full Text Show Details
Sachs
Patent: DE104624 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 5, p. 926