反应条件
in acetonitrile inert atmosphere, Schlenk techniques; aq. Na(pic) soln. addn. to stirred mixt. of V-compd., NaO2CEt and MeCN, stirring overnight, NaCl ppt. filtration off, NEt4Cl addn. to filtrate, solvent removal (vac.), residue redissoln. (acetone), THF addn.; pptn. after a few on standing at room temp., ppt. filtration off, washing (THF), vac. drying; elem. anal.;
参考文献
Castro, Stephanie L.; Sun, Ziming; Grant, Craig M.; Bollinger, John C.; Hendrickson, David N.; Christou, George
Journal of the American Chemical Society, 1998 , vol. 120, # 10 p. 2365 - 2375