二乙基三甲基硅基亚磷酸酯合成路线 (共 88 条)
反应条件
T=45 - 55°C; 3 h; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 1673 - 1674
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1830 - 1832
反应条件
T=150°C; 6 h; Mechanism;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
反应条件
bromine T=-60 - -40°C; 6 h; solvent (CH2Cl2) was used as well;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
反应条件
T=-80°C; P=50 Torr; 3 h;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
反应条件
T=150°C; 6 h; Mechanism;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 1.2 p. 217 - 218
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 235 - 237
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 1.2 p. 217 - 218
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 235 - 237
反应条件
sodium perchlorate; sodium salt of phosphorous acid in acetonitrile electrolysis; Product distribution;
参考文献
Romakhin; Kosachev; Nikitin
Russian Journal of General Chemistry, 1996 , vol. 66, # 12 p. 1901 - 1908
反应条件
sodium perchlorate; sodium salt of phosphorous acid in acetonitrile electrolysis; Product distribution;
参考文献
Romakhin; Kosachev; Nikitin
Russian Journal of General Chemistry, 1996 , vol. 66, # 12 p. 1901 - 1908
反应条件
sodium perchlorate; sodium salt of phosphorous acid in acetonitrile electrolysis; Product distribution;
参考文献
Romakhin; Kosachev; Nikitin
Russian Journal of General Chemistry, 1996 , vol. 66, # 12 p. 1901 - 1908