二(4-溴苯基)碘鎓三氟甲烷磺酸盐合成路线 (共 8 条)
反应条件
triethylamine; copper(l) chloride in dichloromethane T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183
反应条件
[Cu(I)(CH3CN)4]PF6; N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; 16 h; Inert atmosphereSchlenk techniqueIrradiation;
参考文献
Baralle, Alexandre; Fensterbank, Louis; Goddard, Jean-Philippe; Ollivier, Cyril
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 10809 - 10813
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile T=25°C; 12 h; Inert atmosphereIrradiationSchlenk technique;
参考文献
Liu, Yu-Xia; Xue, Dong; Wang, Jia-Di; Zhao, Cong-Jun; Zou, Qing-Zhu; Wang, Chao; Xiao, Jianliang
Synlett, 2013 , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane T=70°C; 72 h; regioselective reaction;
参考文献
Ciana, Claire-Lise; Phipps, Robert J.; Brandt, Jochen R.; Meyer, Falco-Magnus; Gaunt, Matthew J.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 2 p. 458 - 462
反应条件
potassium thiocyanate in neat (no solvent) T=120°C; 0.166667 h; Microwave irradiation;
参考文献
Vaddula, Buchi Reddy; Varma, Rajender S.; Leazer, John
European Journal of Organic Chemistry, 2012 , # 35 p. 6852 - 6855
反应条件
in neat (no solvent) T=150°C; 1 h; Inert atmosphereMicrowave irradiation; Overall yield = 69 percent; Overall yield = 98 mg;
参考文献
Castro, Susana; Fernandez, Juan J.; Vicente, Ruben; Fananas, Francisco J.; Rodriguez, Felix
Chemical Communications, 2012 , vol. 48, # 72 p. 9089 - 9091
反应条件
in neat (no solvent) T=150°C; 1 h; Inert atmosphereMicrowave irradiation; Overall yield = 69 percent; Overall yield = 98 mg;
参考文献
Castro, Susana; Fernandez, Juan J.; Vicente, Ruben; Fananas, Francisco J.; Rodriguez, Felix
Chemical Communications, 2012 , vol. 48, # 72 p. 9089 - 9091
反应条件
triethylamine; copper(l) chloride in dichloromethane
T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183