CH3MgBr in diethyl ether evapn. of the ether; heating of the residue in water-bath for a few hours;;
参考文献
Whitmore, F. C.; Sommer, L. H.; Giorgio, P. A. di; Strong, W. A.; Strien, R. E. van; et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 475 - 481
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Gmelin Handbook: Si: MVol.C, 9, page 28 - 32