1,1,1,2,2,2-hexabutyl-distannane; benzene sulphinic acid in benzene-d6 T=120°C; 12 h;
参考文献
Markovic, Dean; Varela-Alvarez, Adrian; Sordo, Jose Angel; Vogel, Pierre
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 7782 - 7795
n-butyllithium in hexane n-BuLi (1.50 mmol, 2.40 M soln. in hexane) added to soln. of TMTH (1.50 mmol) in hexane under Ar, stirred for 3 h at room temp., 1-bromoheptane (1.50 mmol) added, heated to reflux for 2 h; analyzed by GC;
formic acid; 1,3-bis(2,4,6-trimethylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene; triethylamine; [Pd(1,4-di-t-butyl-1,4-diazabutadiene)(maleic anhydride)] in para-xylene; acetonitrile Heating; Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 17 p. 3223 - 3226
