1-苯硫基-吡咯啉-2,5-二酮合成路线 (共 38 条)
反应条件
palladium diacetate; trifluoroacetic acid T=20°C; 0.75 h; SolventTimeReagent/catalystConcentration;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
1: 72 percent / BF3*Et2O / CH2Cl2 / 4 h / 20 - 45 °C 2: 69 percent / aq. NH3; NH4Cl / 100 °C View Scheme
参考文献
Silvestri, Romano; De Martino, Gabriella; La Regina, Giuseppe; Artico, Marino; Massa, Silvio; Vargiu, Laura; Mura, Massimo; Loi, Anna Giulia; Marceddu, Tiziana; La Colla, Paolo
Journal of Medicinal Chemistry, 2003 , vol. 46, # 12 p. 2482 - 2493
反应条件
in benzene 20 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 695 - 698
反应条件
in benzene 20 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 695 - 698
反应条件
in benzene 20 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 695 - 698
反应条件
1: triethylamine / dichloromethane / 24 h / 20 °C 2: sodium tetrahydroborate / methanol / 0.33 h / 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 20 °C 4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 5: hexane; dichloromethane / 1 h / 0 - 20 °C View Scheme
参考文献
Shimada, Hisashi; Kikuchi, Satoshi; Okuda, Saori; Haraguchi, Kazuhiro; Tanaka, Hiromichi
Tetrahedron, 2009 , vol. 65, # 31 p. 6008 - 6016
反应条件
1: boron trifluoride diethyl etherate / CH2Cl2 / 3.5 h / 20 - 45 °C 2: 3-chloroperoxybenzoic acid / CHCl3 / 1.3 h / 20 °C View Scheme
参考文献
Silvestri, Romano; De Martino, Gabriella; La Regina, Giuseppe; Artico, Marino; Massa, Silvio; Vargiu, Laura; Mura, Massimo; Loi, Anna Giulia; Marceddu, Tiziana; La Colla, Paolo
Journal of Medicinal Chemistry, 2003 , vol. 46, # 12 p. 2482 - 2493
反应条件
in toluene Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
反应条件
scandium tris(trifluoromethanesulfonate) in water T=30°C; 6 h; Ionic liquid; Catalytic behavior; Reagent/catalyst;
参考文献
Liang, Gaigai; Chen, Jing; Chen, Jiali; Li, Wanmei; Chen, Jiuxi; Wu, Huayue
Tetrahedron Letters, 2012 , vol. 53, # 50 p. 6768 - 6770
反应条件
scandium tris(trifluoromethanesulfonate) in water T=30°C; 2 h; Ionic liquid;
参考文献
Liang, Gaigai; Chen, Jing; Chen, Jiali; Li, Wanmei; Chen, Jiuxi; Wu, Huayue
Tetrahedron Letters, 2012 , vol. 53, # 50 p. 6768 - 6770