N-(2-羟乙基)对甲苯磺酰胺合成路线 (共 22 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 18 h; Inert atmosphere;
参考文献
Law, Katherine R.; McErlean, Christopher S. P.
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15852 - 15855
反应条件
in ethanol; water T=20°C; 6.16667 h; chemospecific reaction;
参考文献
Verma, Sanjeev K.; Acharya; Kaushik
Organic Letters, 2010 , vol. 12, # 19 p. 4232 - 4235
反应条件
cesium fluoride supported on Celite T=50°C; chemoselective reaction;
参考文献
Tamaddon, Fatemeh; Nasiri, Alireza; Farokhi, Somayeh
Catalysis Communications, 2011 , vol. 12, # 15 p. 1477 - 1482
反应条件
N-Trimethylamine hydrochloride; triethylamine in dichloromethane; toluene T=0°C; 1 h;
参考文献
Heterocycles, , vol. 63, # 10 p. 2269 - 2285
反应条件
1: With [bis(acetoxy)iodo]benzene; copper(II) bis(trifluoromethanesulfonate) in dichloromethane T=40°C; 4 h; 2: With sodium tetrahydroborate in tetrahydrofuran T=25°C; Further stages.;
参考文献
Organic Letters, , vol. 9, # 12 p. 2277 - 2280
反应条件
1: N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-methyl-benzenesulfonamide With sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; 1.5 h; Inert atmosphere; 2: methyl (2E,4E)-6-bromo-2,4-hexadienoate in tetrahydrofuran; mineral oil T=20°C; 20 h; Inert atmosphere; 3: With acetic acid in tetrahydrofuran; water T=20°C; 18 h; Inert atmosphere;
参考文献
Law, Katherine R.; McErlean, Christopher S. P.
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15852 - 15855
反应条件
1: 4-hydroxybutanol; p-toluenesulfonyl chloride With triethylamine in dichloromethane 25.25 h; Inert atmosphere; 2: ethanolamine in dichloromethane
参考文献
Hoogenboom, Richard; Fijten, Martin W. M.; Kickelbick, Guido; Schubert, Ulrich S.
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, p. 773 - 783
反应条件
triethylamine in dichloromethane T=0 - 20°C; 16.5 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 3 p. 872 - 885
反应条件
pyridine T=0 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 75, # 10 p. 3515 - 3517
反应条件
1: dirhodium(II) tetraoctanoate; water / chloroform / 0.25 h / 140 °C / Microwave irradiation 2: sodium tetrahydroborate / ethanol; water View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 1 p. 194 - 196