N-苯基-氨基磷酸二乙酯合成路线 （共 38 条）
反应条件
potassium carbonate; potassium hydrogencarbonate; tetrabutylammomium bromide in tetrachloromethane T=15 - 20°C; 4 h;
参考文献
Zwierzak, Andrzej; Osowska, Krystyna
Synthesis, 1984 , # 3 p. 223 - 224
反应条件
1: in dichloromethane T=27°C; Staudinger phosphite reaction; 2: With water in dichloromethane T=27°C; 24 h; chemoselective reaction;
参考文献
Serwa, Remigiusz; Wakening, Lna; Signore, Giuseppe Del; Muehlberg, Michaela; Claussnitzer, Iris; Weise, Christoph; Gerrits, Michael; Hackenberger, Christianr P. R.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8234 - 8239
反应条件
potassium carbonate; potassium hydrogencarbonate; tetrabutylammomium bromide in tetrachloromethane; dichloromethane T=15 - 20°C; 4 h;
参考文献
Zwierzak, Andrzej; Osowska, Krystyna
Synthesis, 1984 , # 3 p. 223 - 224
反应条件
in toluene T=200°C; P=15001.5 Torr; 0.25 h; Microwave irradiation;
参考文献
Haggam, Reda; Conrad, Juergen; Beifuss, Uwe
Tetrahedron Letters, 2009 , vol. 50, # 48 p. 6627 - 6630
反应条件
sodium hydroxide; phenylmethyltriethylammonium bromide in tetrachloromethane 1.) 0 deg C, 1 h, 2.) room temp., 4 h;
参考文献
Lukanov, L. K.; Venkov, A. P.; Mollov, N. M.
Synthesis, 1985 , # 10 p. 971 - 973
反应条件
sodium hydroxide; phenylmethyltriethylammonium bromide in tetrachloromethane 1.) 0 deg C, 1 h, 2.) room temp., 4 h;
参考文献
Lukanov, L. K.; Venkov, A. P.; Mollov, N. M.
Synthesis, 1985 , # 10 p. 971 - 973
反应条件
triethylamine in benzene 96 h; Ambient temperature;
参考文献
Moody, Christopher J.; Rees, Charles W.; Thomas, Robert
Tetrahedron, 1992 , vol. 48, # 17 p. 3589 - 3602
反应条件
water in diethyl ether 1.5 h;
参考文献
Kamalov, R. M.; Khailova, N. A.; Al'fonsov, V. A.; Pudovik, M. A.
Russian Journal of General Chemistry, 1995 , vol. 65, # 1.1 p. 37 - 42
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 1 p. 46 - 52
反应条件
in benzene 0.5 h; Ambient temperaturefurther educts: O,O'-diethylphosphoric trifluoromethane, -imidazolidosulfuric, -4-methylbenzenesulfonic anhydrides;
参考文献
Dabkowski, Wojciech; Michalski, Jan; Skrzypczynski, Zbigniew
Chemische Berichte, 1985 , vol. 118, # 5 p. 1809 - 1824
反应条件
in benzene 1 h; Ambient temperature;
参考文献
Dabkowski, Wojciech; Michalski, Jan; Radziejewski, Czeslaw; Skrypczynski, Zbigniew
Chemische Berichte, 1982 , vol. 115, # 4 p. 1636 - 1643
