N-2-丙炔基-苯甲酰胺合成路线 （共 33 条）
反应条件
triethylamine in dichloromethane T=20°C; 1 h;
参考文献
Wipf, Peter; Aoyama, Yasunori; Benedum, Tyler E.
Organic Letters, 2004 , vol. 6, # 20 p. 3593 - 3595
反应条件
triethylamine in dichloromethane T=20°C; 18 h; Inert atmosphere;
参考文献
Andrade, Gabriel A.; Pistner, Allen J.; Yap, Glenn P. A.; Lutterman, Daniel A.; Rosenthal, Joel
ACS Catalysis, 2013 , vol. 3, # 8 p. 1685 - 1692
反应条件
1: monopropargylamine With bis(trimethylaluminum)-1,4-diazabicyclo[2.2.2]octane in tetrahydrofuran T=40°C; 1 h; 2: benzoic acid methyl ester in tetrahydrofuran 18 h; Heating;
参考文献
Novak, Andrew; Humphreys, Luke D.; Walker, Matthew D.; Woodward, Simon
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5767 - 5769
反应条件
potassium tert-butylate in dimethyl sulfoxide T=110°C; 8 h;
参考文献
Yasmin, Nasima; Ray, Jayanta K.
Synlett, 2009 , # 17 p. 2825 - 2827
反应条件
in dichloromethane T=20°C; 48 h;
参考文献
Botta, Maurizio; Corelli, Federico; Petricci, Elena; Seri, Catia
Heterocycles, 2002 , vol. 56, # 1-2 p. 369 - 377
参考文献
Yi, Jun; Lu, Xi; Sun, Yan-Yan; Xiao, Bin; Liu, Lei
Angewandte Chemie - International Edition, 2013 , vol. 52, # 47 p. 12409 - 12413
Angew. Chem., 2013 , vol. 125, # 47 p. 12635 - 12639,5
反应条件
Ru(phen)3(Cl)2; oxygen in dimethyl sulfoxide T=32°C; 72 h; IrradiationSchlenk technique;
参考文献
Liu, Jie; Liu, Qiang; Yi, Hong; Qin, Chu; Bai, Ruopeng; Qi, Xiaotian; Lan, Yu; Lei, Aiwen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 502 - 506
Angew. Chem., 2014 , vol. 126, # 2 p. 512 - 516,5
反应条件
1: dicyclohexyl-carbodiimide / tetrahydrofuran / 20 h / 20 °C 2: triethylamine / dichloromethane / 18 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Andrade, Gabriel A.; Pistner, Allen J.; Yap, Glenn P. A.; Lutterman, Daniel A.; Rosenthal, Joel
ACS Catalysis, 2013 , vol. 3, # 8 p. 1685 - 1692
反应条件
1: N-(prop-2-yn-1-yl)benzamide With sodium hydride in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: allyl bromide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Hashmi, A. Stephen K.; Molinari, Lise; Rominger, Frank; Oeser, Thomas
European Journal of Organic Chemistry, 2011 , # 12 p. 2256 - 2264
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in acetonitrile T=90°C;
参考文献
Saito, Akio; Iimura, Koichi; Hanzawa, Yuji
Tetrahedron Letters, 2010 , vol. 51, # 11 p. 1471 - 1474
