4-乙酰氨基-TEMPO合成路线 （共 10 条）
反应条件
sodium tungstate; dihydrogen peroxide; tetrasodium ethylenediaminetetraacetate; potassium carbonate in water 72 h;
参考文献
Bobbitt, James M.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9367 - 9374
反应条件
NaBO3; dihydrogen peroxide; potassium carbonate in water 24 h; Ambient temperature;
参考文献
Ma, Zhenkun; Bobbitt, James M.
Journal of Organic Chemistry, 1991 , vol. 56, # 21 p. 6110 - 6114
反应条件
1.1: 197 g / diethyl ether / 3.5 h / 5 - 10 °C 2.1: K2CO3 / H2O / 0.25 h / 25 °C 2.2: 150.8 g / H2O2; sodium tungstate; disodium EDTA / H2O / 73 h View Scheme
参考文献
Monatshefte fur Chemie, , vol. 134, # 6 p. 843 - 850
参考文献
Kashparova; Kagan; Kashparov; Zhukova
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 4 p. 667 - 668
参考文献
Carbohydrate research, , vol. 89, # 2 p. 211 - 220
反应条件
1: piperidine; 5-phenyl benzoxazole With scandium tris(trifluoromethanesulfonate) in acetonitrile T=60°C; 6 h; 2: oxoammonium salt With 2,2,6,6-tetramethyl-piperidine in acetonitrile T=60°C; 0.166667 h;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 48 p. 11511 - 11515
反应条件
1: 49 percent / KOH / H2O / 29 h / Heating 2: 67 percent / Et3N / benzene / 20 °C View Scheme
参考文献
Plessas; Goldstein
Carbohydrate research, 1981 , vol. 89, # 2 p. 211 - 220
参考文献
Fritz-Langhals, Elke; Stohrer, Juergen; Petersen, Hermann
Patent: US2003/73871 A1, 2003 ;
反应条件
potassium hydroxide in methanol; water T=100°C; 96 h; Sealed tube;
参考文献
Dickschat, Arne T.; Surmiak, Sabrina; Studer, Armido
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-B0314-L, p. 1523 - 1528
参考文献
Labsky, J.; Pilar, J.; Loevy, J.
Journal of Magnetic Resonance (1969-1992), 1980 , vol. 37, # 3 p. 515 - 522
