3,4-亚甲二氧-beta-硝基苯乙烯合成路线 （共 27 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20 - 70°C; 4 h;
参考文献
Koseki, Yuji; Katsura, Shinya; Kusano, Shuichi; Sakata, Harumi; Sato, Hiroto; Monzene, Yoshinori; Nagasaka, Tatsuo
Heterocycles, 2003 , vol. 59, # 2 p. 527 - 540
参考文献
Gensler; Samour
Journal of the American Chemical Society, 1951 , vol. 73, p. 5555
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Erne; Ramirez
Helvetica Chimica Acta, 1950 , vol. 33, p. 912,915
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Benington et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1979,1980
参考文献
Gensler; Samour
Journal of the American Chemical Society, 1951 , vol. 73, p. 5555
Full Text View citing articles Show Details
Erne; Ramirez
Helvetica Chimica Acta, 1950 , vol. 33, p. 912,915
Full Text Show Details
Benington et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1979,1980
参考文献
Gensler; Samour
Journal of the American Chemical Society, 1951 , vol. 73, p. 5555
Full Text View citing articles Show Details
Erne; Ramirez
Helvetica Chimica Acta, 1950 , vol. 33, p. 912,915
Full Text Show Details
Benington et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1979,1980
参考文献
Kindler; Brandt
Archiv der Pharmazie (Weinheim, Germany), 1935 , vol. 273, p. 478,482
Full Text Show Details
Schales
Chemische Berichte, 1935 , vol. 68, p. 1579,1581
反应条件
bei der elektrolytischen Reduktion;
参考文献
Bayer and Co.
Patent: DE254861 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 1006
参考文献
Kondo et al.
Itsuu Kenkyusho Nempo, 1951 , # 2 p. 11; dtsch. Ref. S. 48
Chem.Abstr., 1953 , p. 7519
参考文献
Bayer and Co.
Patent: DE245523 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 1192
反应条件
1: 78 percent / DBU / tetrahydrofuran; propan-2-ol / 4 h / Ambient temperature 2: 12.34 g / H2 / Raney nickel / ethanol / 3040 Torr 3: 1.) sodium cyanoborohydride, 2.) bromocresol green, conc. HCl / 1.) THF, EtOH, 2.) THF, EtOH, 20 min 4: 2.775 g / C2H5ONa / ethanol / Heating 5: 91 percent / CH2Cl2 / 1 h / Ambient temperature 6: 95 percent / NaOH 7: 1.) Et3N, t-BuCOCl, 2.) n-BuLi 8: 4 N aq. HCl / dioxane 9: iPr2NEt / acetonitrile 10: 78 percent / aq. LiOH, 30percent aq. H2O2 / tetrahydrofuran / 0.5 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 5 p. 1039 - 1048
反应条件
1: 82 percent / MeOH / benzene / 0.08 h / 0 - 5 °C
2: LiAlH4, conc. H2SO4 / tetrahydrofuran / 1.) RT, 30 min, 2.) reflux, 2 h
View Scheme
参考文献
Torres; Cassels; Rezende
Synthetic Communications, 1995 , vol. 25, # 8 p. 1239 - 1247
