oxygen; NHS; Co(acetylacetonate)3 in various solvent(s) T=100°C; P=760.051 Torr; 5 h;
参考文献
Baucherel, Xavier; Gonsalvi, Luca; Arends, Isabel W. C. E.; Ellwood, Simon; Sheldon, Roger A.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 2-3 p. 286 - 296
in tetrahydrofuran addn. of CH2Cl2 to soln. of B-methoxyborecane in THF, cooling to -78°C, slow addn. of sec-BuLi over period of 0.5 h, stirred at -78°C for 0.25 h, addn. of KIPBH, warmed to room temp, stirred for 14 h;; GLC, amt. of cyclodecanol formed depends upon temp. during the addn. of KIPBH;;
参考文献
Brown, Herbert C.; Phadke, Avinash S.; Rangaishenvi, Milind V.
Journal of the American Chemical Society, 1988 , vol. 110, # 18 p. 6263 - 6264
