3-甲基-4-戊烯-2-醇合成路线 （共 10 条）
反应条件
in diethyl ether
T=-5°C;
参考文献
Ashcroft, Martyn R.; Bury, Adrian; Cooksey, Christopher J.; Davies, Alwyn G.; Gupta, B. Dass; et al.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 89 - 104
反应条件
magnesium
anschliessend mit Acetaldehyd in Aether;
参考文献
Roberts; Young
Journal of the American Chemical Society, 1945 , vol. 67, p. 150
Full Text Show Details
Ou
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1939 , vol. 208, p. 529
Annales de Chimie (Cachan, France), 1940 , vol. <11>13, p. 191
Full Text Show Details
Kharasch,M.S.; Reinmuth,O.
Grignard Reactions of Nonmetallic Substances <New York>S.1149-1157
反应条件
boron trifluoride diethyl etherate
T=-20°C; Yield given;
参考文献
Denmark, Scott E.; Weber, Eric J.; Wilson, Thomas M.; Willson, Timothy M.
Tetrahedron, 1989 , vol. 45, # 4 p. 1053 - 1066
反应条件
dihydrogen peroxide in tetrahydrofuran
under nitrogen, cooled at 0°C, after stirring for 45 min NaOH (3 M) and 30percent H2O2 added, stirred for 1 h, water added, saturated with K2CO3; aq. phase extn. (ether), combined org. phase dried, destn. under vacuum; NMR;
参考文献
Hill, E. Alexander; Park, Young-Whan
Journal of Organometallic Chemistry, 1988 , vol. 356, p. 1 - 16
反应条件
aluminium trichloride
1.) ether, -78 deg C, 10 min, 2.) -78 deg C to 0 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yamamoto, Yoshinori; Maruyama, Kazuhiro
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1564 - 1565
参考文献
Colonge,J. et al.
Bulletin de la Societe Chimique de France, 1965 , p. 619 - 625
反应条件
(i), (ii) (HOCH2CH2)3N; Multistep reaction;
参考文献
Mikhailov,B.M. et al.
Journal of Organometallic Chemistry, 1978 , vol. 154, p. 131 - 145
参考文献
Roberts; Young
Journal of the American Chemical Society, 1945 , vol. 67, p. 150
Full Text Show Details
Ou
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1939 , vol. 208, p. 529
Annales de Chimie (Cachan, France), 1940 , vol. <11>13, p. 191
Full Text Show Details
Kharasch,M.S.; Reinmuth,O.
Grignard Reactions of Nonmetallic Substances <New York 1954>S.1149-1157
反应条件
analog reagiert mit anderen Aldehyden und mit Aceton;
参考文献
Roberts; Young
Journal of the American Chemical Society, 1945 , vol. 67, p. 150
Full Text Show Details
Ou
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1939 , vol. 208, p. 529
Annales de Chimie (Cachan, France), 1940 , vol. <11>13, p. 191
参考文献
Tolstikov, G. A.; Spivak, A. Yu.; Lomakina, S. I.; Kuchin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 5 p. 1012 - 1017
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 5 p. 1109 - 1114
