反应条件
in pentane (N2); addn. of excess SCCl2 to Mn-complex in pentane, stirring (10 min, 0°C), stirring (30 min, room temp.); filtration, evapn. to dryness, sublimation (high vac., 30-40°C), chromy. (Al2O3, pentane); product mixt. not sepd.; total yield 12-14percent;
参考文献
Petz; Rehder
Organometallics, 1990 , vol. 9, # 3 p. 856 - 859