2,3-二甲基-5-乙基吡嗪合成路线 (共 39 条)
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; Negishi coupling reaction; 12 h; Inert atmosphere;
参考文献
Pitchaiah, Arigala; Hwang, Intaek; Hwang, Jin-Soo; Kim, Hyungrok; Lee, Kee-In
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-F0234-OP, p. 1631 - 1636
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; 12 h; Inert atmosphere;
参考文献
Pitchaiah, Arigala; Hwang, Intaek; Hwang, Jin-Soo; Kim, Hyungrok; Lee, Kee-In
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-F0234-OP, p. 1631 - 1636
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; 12 h; Inert atmosphere;
参考文献
Pitchaiah, Arigala; Hwang, Intaek; Hwang, Jin-Soo; Kim, Hyungrok; Lee, Kee-In
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-F0234-OP, p. 1631 - 1636
反应条件
in toluene T=300°C; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 8 p. 2605 - 2606
反应条件
1: potassium tert-butoxide / dimethylsulfoxide / 2 h / 50 °C 2: Et3N / CH2Cl2 / 10 - 20 °C 3: toluene / 300 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 8 p. 2605 - 2606
反应条件
1: Et3N / CH2Cl2 / 10 - 20 °C 2: toluene / 300 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 8 p. 2605 - 2606
反应条件
1: pyridine / chloroform / 2.5 h / -78 - 20 °C / Inert atmosphere 2: [1,3-bis(diphenylphosphino) propane] dichloronickel(II) / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Synthesis (Germany), , vol. 44, # 11 art. no. SS-2012-F0234-OP, p. 1631 - 1636
反应条件
in water T=130°C; Maillard reaction; pH=8; 2 h;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 4 p. 2470 - 2478
反应条件
sodium hydroxide T=143°C; Maillard reaction; pH=9.55; 2 h; aq. phosphate bufferSealed vial;
参考文献
Food Chemistry, , vol. 119, # 1 p. 214 - 219
反应条件
sodium hydroxide T=143°C; Maillard reaction; pH=8; 2 h; aq. phosphate bufferSealed vial;
参考文献
Food Chemistry, , vol. 119, # 1 p. 214 - 219