2-溴-4-氯-6-硝基苯酚合成路线 （共 19 条）
参考文献
Kohn; Krasso
Journal of Organic Chemistry, 1946 , vol. 11, p. 641,644
参考文献
Gordon
Chem. News J. Ind. Sci., 1891 , vol. 63, p. 222
Chem. Zentralbl., 1891 , vol. 62, # I p. 1031
参考文献
Upson
American Chemical Journal, 1904 , vol. 32, p. 15
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Ling
Journal of the Chemical Society, 1887 , vol. 51, p. 786
Journal of the Chemical Society, 1892 , vol. 61, p. 577
反应条件
1: sodium carbonate; palladium diacetate / water / 3.5 h / 50 °C / |Inert atmosphere 2: hydrogen; palladium 10 on activated carbon; triethylamine / methanol / 21 h / 20 °C / 7500.75 Torr / |Autoclave View Scheme
参考文献
ASSIA CHEMICAL INDUSTRIES LTD.; TEVA PHARMACEUTICAL USA, INC.; AVDAGIC, Amir; BARAN, Phil, S.
Patent: WO2013/49605 A1, 2013 ;
反应条件
palladium diacetate; sodium carbonate in water T=50°C; 3.5 h; Inert atmosphere;
参考文献
ASSIA CHEMICAL INDUSTRIES LTD.; TEVA PHARMACEUTICAL USA, INC.; AVDAGIC, Amir; BARAN, Phil, S.
Patent: WO2013/49605 A1, 2013 ;
Location in patent: Paragraph 0055 ;
参考文献
Ling
Journal of the Chemical Society, 1887 , vol. 51, p. 786
Journal of the Chemical Society, 1892 , vol. 61, p. 577
反应条件
hydrogen; Raney Ni in ethyl acetate 4 h;
参考文献
KHAMRAI, Uttam; Ronsheim, Matthew; Karak, Sumit Kumar
Patent: US2010/152160 A1, 2010 ;
Location in patent: Page/Page column 111 ;
US 20100152160 A1
参考文献
Euro-Celtique S.A.
Patent: EP1160247 A1, 2001 ;
参考文献
Ling
Journal of the Chemical Society, 1889 , vol. 55, p. 585,587
