cesium carbonate in isopropyl alcohol
under Ar; i-PrOH added to mixt. of Hg acetate, B compd. and Cs2CO3; sealed; heated at 50-55°C (oil bath) for 12-20 h; cooled; solvent removed by rotary evapn.; extd. with toluene or toluene-THF; filtered; filtrate reduced to dryness by rotary evapn.; triturated with pentane; dried; elem. anal.;
参考文献
Partyka, David V.; Gray, Thomas G.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 2 p. 213 - 218
