磷酸二乙基(2-氯苯基)酯合成路线 (共 5 条)
反应条件
magnesium oxide T=20°C; Solid phase reaction; 0.5 h;
参考文献
Kaboudin
Journal of Chemical Research - Part S, 1999 , # 6 p. 402 - 403
反应条件
tetrachloromethane; chlorine Behandeln des Reaktionsprodukts mit 2-Chlor-phenol und wss. Natronlauge;
参考文献
Orloff et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 727,729
反应条件
buffer: tris(hydroxymethyl)aminomethane in 1,4-dioxane; water T=25°C; pH 7.91, 0.5 M ionic strength; Rate constant;
参考文献
Ba-Saif, Salem; Williams, Andrew
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2204 - 2209
反应条件
sodium hydroxide; chlorine 1.) CCl4, 0 deg C; 2.) H2O, room temp., 2 h; Yield given. Multistep reaction;
参考文献
Heinicke, J.; Boehle, I.; Tzschach, A.
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 11 - 22
反应条件
sodium in 1,4-dioxane
1.) 40 deg C, 5 h, 2.) r.t., overnight;
参考文献
Li, Shusen; Wang, Guoquan
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 61, # 12 p. 119 - 129