1-甲氧基-2-(4-甲氧基苯氧基)苯合成路线 (共 14 条)
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(l) chloride in 1-methyl-pyrrolidin-2-one T=120°C; Ullmann reaction; 25 h;
参考文献
Buck, Elizabeth; Song, Zhiguo Jake; Tschaen, David; Dormer, Peter G; Volante; Reider, Paul J
Organic letters, 2002 , vol. 4, # 9 p. 1623 - 1626
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(l) chloride in 1-methyl-pyrrolidin-2-one T=120°C; Ullmann reaction; 15 h;
参考文献
Buck, Elizabeth; Song, Zhiguo Jake; Tschaen, David; Dormer, Peter G; Volante; Reider, Paul J
Organic letters, 2002 , vol. 4, # 9 p. 1623 - 1626
反应条件
copper diacetate; 4 A molecular sieve; triethylamine in dichloromethane T=25°C; 18 h;
参考文献
Evans, David A.; Katz, Jeffrey L.; West, Theodore R.
Tetrahedron Letters, 1998 , vol. 39, # 19 p. 2937 - 2940
反应条件
copper T=220 - 230°C;
参考文献
Sartoretto; Sowa
Journal of the American Chemical Society, 1937 , vol. 59, p. 603
反应条件
1: aq. NaOH 3: H2 / Pt 4: (i) aq. NaNO2, aq. HCl, (ii) aq. H3PO2 View Scheme
参考文献
Govindachari,T.R. et al.
Indian Journal of Chemistry, 1966 , vol. 4, p. 433 - 437
反应条件
2: H2 / Pt 3: (i) aq. NaNO2, aq. HCl, (ii) aq. H3PO2 View Scheme
参考文献
Govindachari,T.R. et al.
Indian Journal of Chemistry, 1966 , vol. 4, p. 433 - 437
反应条件
1: H2 / Pt 2: (i) aq. NaNO2, aq. HCl, (ii) aq. H3PO2 View Scheme
参考文献
Govindachari,T.R. et al.
Indian Journal of Chemistry, 1966 , vol. 4, p. 433 - 437
反应条件
(i) aq. NaNO2, aq. HCl, (ii) aq. H3PO2; Multistep reaction;
参考文献
Govindachari,T.R. et al.
Indian Journal of Chemistry, 1966 , vol. 4, p. 433 - 437
参考文献
Sartoretto; Sowa
Journal of the American Chemical Society, 1937 , vol. 59, p. 603
参考文献
Tomita; Watanabe
Yakugaku Zasshi, 1953 , vol. 73, p. 918
Chem.Abstr., 1954 , p. 10652