二乙氧基磷酰-苯基-甲醇合成路线 （共 37 条）
反应条件
trimethylphosphane in tetrahydrofuran
T=20°C; 2 h;
参考文献
Zhang, Wen; Shi, Min
Chemical Communications, 2006 , # 11 p. 1218 - 1220
反应条件
Cp2Zr(OSO2C4H9)2*2H2O in neat (no solvent)
T=20°C; Kabachnik-Fields Reaction; 8 h;
参考文献
Li, Ningbo; Wang, Xie; Qiu, Renhua; Xu, Xinhua; Chen, Jinyang; Zhang, Xiaohong; Chen, Sihai; Yin, Shuangfeng
Catalysis Communications, 2014 , vol. 43, p. 184 - 187
反应条件
Cp2Zr(OSO2C4H9)2*2H2O in neat (no solvent)
T=20°C; Kabachnik-Fields Reaction; 10 h;
参考文献
Li, Ningbo; Wang, Xie; Qiu, Renhua; Xu, Xinhua; Chen, Jinyang; Zhang, Xiaohong; Chen, Sihai; Yin, Shuangfeng
Catalysis Communications, 2014 , vol. 43, p. 184 - 187
反应条件
Cp2Zr(OSO2C4H9)2*2H2O in neat (no solvent)
T=20°C; Kabachnik-Fields Reaction; 10 h;
参考文献
Li, Ningbo; Wang, Xie; Qiu, Renhua; Xu, Xinhua; Chen, Jinyang; Zhang, Xiaohong; Chen, Sihai; Yin, Shuangfeng
Catalysis Communications, 2014 , vol. 43, p. 184 - 187
反应条件
1: phosphorous acid diethyl ester With [(Me3Si)2N]3La(μ-Cl)Li(THF)3 in toluene
Pudovik reaction; 0.166667 h; Inert atmosphere;
2: benzaldehyde in toluene
T=25°C; Pudovik reaction; 0.0833333 h; Inert atmosphere;
参考文献
Wu, Qingmao; Zhou, Jun; Yao, Zhigang; Xu, Fan; Shen, Qi
Journal of Organic Chemistry, 2010 , vol. 75, # 21 p. 7498 - 7501
参考文献
Novikova,Z.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 2622 - 2628,2655 - 2660
反应条件
in toluene
2 h; Reflux;
参考文献
Kaboudin, Babak; Karami, Leila; Kato, Jun-Ya; Aoyama, Hiroshi; Yokomatsu, Tsutomu
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4872 - 4875
反应条件
hydrogenchloride in diethyl ether; dichloromethane
T=-10°C; 1 h;
参考文献
Goldeman, Waldemar; Soroka, Miroslaw
Synthesis, 2006 , # 18 p. 3019 - 3024
反应条件
benzaldehyde in methanol
参考文献
The Upjohn Company
Patent: US5500417 A1, 1996 ;
反应条件
10 Pd/C; hydrogen in methanol
T=65°C; P=750.075 Torr; 2 h; Inert atmosphere;
参考文献
Goulioukina, Nataliya S.; Bondarenko, Grigorii N.; Lyubimov, Sergey E.; Davankov, Vadim A.; Gavrilov, Konstantin N.; Beletskaya, Irina P.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 3 p. 482 - 492
