二乙氧基磷酰-苯基-甲醇合成路线 （共 37 条）
反应条件
phosphorous acid diethyl ester
0.333333 h; Ambient temperature;
参考文献
Gancarz, Roman
Tetrahedron, 1995 , vol. 51, # 38 p. 10627 - 10632
反应条件
24 h; Ambient temperature;
参考文献
Gancarz, Roman
Tetrahedron, 1995 , vol. 51, # 38 p. 10627 - 10632
反应条件
sodium hydroxide
1.) THF, -78 deg C, 2.) water, -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Longmire, Cynthia F.; Evans, Slayton A.
Journal of the Chemical Society, Chemical Communications, 1990 , # 13 p. 922 - 923
参考文献
Kabatschnik; Rossiiskaja
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1945 , p. 364,371
Chem.Abstr., 1946 , p. 4688
反应条件
phosphorus pentachloride in tetrachloromethane
15 h; Heating;
参考文献
Collins, David J.; Drygala, Peter F.; Swan, John M.
Australian Journal of Chemistry, 1984 , vol. 37, # 5 p. 1009 - 1021
反应条件
1.1: Ph3P; EtO2C-N=N-CO2Et; HN3 / CH2Cl2 / 20 h / -10 - 20 °C
2.1: tetrahydrofuran / 20 °C
2.2: H2O / tetrahydrofuran / Heating
View Scheme
参考文献
Gajda, Tadeusz; Sikora, Dorota; Nonas, Tomasz
Phosphorus, Sulfur and Silicon and Related Elements, 1999 , vol. 144-146, p. 581 - 584
反应条件
tetrachloromethane; triphenylphosphine
T=80°C; 8 h; Inert atmosphere;
参考文献
Wu, Di; He, Yanhong; Tang, Rongchang; Guan, Zhi
Synlett, 2009 , # 13 p. 2180 - 2182
